Removal of pollutants in the exhaust system was an interesting field and it was inspired by the invention of modern Catalytic Converter (CATCO). The problem is low emission conversion from CO, NOx and HC to H2O, CO2 and NO2 due to low CATCO material conductivity. Therefore, the objective of this research is to investigate the conductivity and resistivity of FeCrAl material for CATCO that coated by combined technique of electroplating and ultrasonic methods. Nickel (Ni) plate as anode and FeCrAl as cathode. The distance between anode and cathode was adjusted at 25 mm. Ultrasonic was carried out using frequency of 35 kHz. Ultrasonic and electroplating were conducted for several variation times of 15, 30, 45, 60 and 75 minutes. Drying process was performed after electroplating process at temperature of 600C for 12 hours. The conductivity and resistivity analysis will be conducted using 4 point probe machine. Resistivity and conductivity analysis show that the smallest resistivity and highest conductivity has been observed at UB+EL 30 minute for 2.67E+03 ohmcm and 3.75E-04 S/cm, respectively. UB samples has lower resistivity and higher conductivity than EL, and UBdEL samples. It may cause by surface roughness of the FrCrAl material that embedded during the coating process.